Thermal analysis & ovens
Differential Scanning Calorimeter (DSC)
Measures the heat flowing into or out of a small sample compared with an empty reference pan while both are heated or cooled. It shows melting, crystallisation, glass transitions and polymorphic changes.
- Pharmaceutical
- Polymers and plastics
- Food
- Materials research
- Chemicals
PREVENTIVE MAINTENANCE
Maintenance checklist
Each use
- Check purge gas flow and pressure
- Inspect the sensor for residue
Weekly / as needed
- Run an indium check if your SOP requires it
- Clean the cell by a bake-out in air as the manufacturer allows
Periodic (as per SOP)
- Temperature and enthalpy calibration with indium (and other standards as needed)
- Baseline calibration
Annual
- Preventive maintenance by the service engineer
- Check of the cooling accessory and gas system
SAFETY
Safety precautions
Before you work on the DSC
- The cell reaches high temperatures; let it cool before opening.
- Handle gas cylinders safely and secure them to a wall or bench.
- Liquid nitrogen cooling needs cryogenic gloves and a face shield.
- Do not run unknown or energetic materials without a risk assessment; they may decompose violently.
In LimsPulse · Calibration Management
Keep every DSC in control: usage logs, calibration and maintenance schedules, and automatic blocking of overdue instruments.