LimsPulse
Thermal analysis & ovens

Melting Point Apparatus

Heats a sample packed in a thin glass capillary at a slow, controlled rate and records the temperatures at which it starts and finishes melting. Used for identity and purity checks of APIs and excipients.

  • Pharmaceutical
  • Fine chemicals
  • Agrochemicals
  • Dyes and pigments
  • Academic labs
Photo of a Melting Point Apparatus
Photo: Iain George, CC BY-SA 2.0 (cropped), via Wikimedia Commons
PREVENTIVE MAINTENANCE

Maintenance checklist

Each use

  • Check the block and capillary holes are clean
  • Check the light and camera image are clear

Monthly

  • Clean the block holes with the cleaning wire supplied
  • Clean the viewing lens or camera window

Periodic (as per SOP)

  • Calibration with melting point reference standards across the working range
  • Check the ramp rate against a stopwatch

Annual

  • Preventive maintenance by a service engineer
  • Check of the temperature sensor and controller
SAFETY

Safety precautions

Before you work on the Melting point apparatus
  • The block can be above 300 °C. Do not touch it and let it cool before cleaning.
  • Glass capillaries are sharp; dispose of them in a sharps container.
  • Some substances give off toxic vapours on melting; work in a ventilated area.
  • Wear safety glasses when packing and handling capillaries.
In LimsPulse · Calibration Management

Keep every Melting point apparatus in control: usage logs, calibration and maintenance schedules, and automatic blocking of overdue instruments.

See how