Physical testing
Microbalance
A very sensitive balance that reads to 0.001 mg (1 µg) or better. It is used when the sample is only a few milligrams, for example a potent reference standard or a DSC sample.
- Pharmaceutical
- Biotech
- Chemicals
- Environmental testing
- Academic research
- Materials science
Follow your site SOP
This is a typical operating sequence for learning. Your instrument model and approved SOP take precedence.
STAGE 1
Before you start
- 1Check the calibration status label, the minimum weight label and that today's check has been done.
- 2Confirm the balance is level (levelling bubble centred).
- 3Check the room: doors closed, no draught from air-conditioning, temperature stable.
- 4Make sure the balance has been powered for the warm-up time the manufacturer states (often several hours for a microbalance; most labs leave it on standby permanently).
- 5Let the sample, container and tools reach room temperature.
- Do not use the balance if it has been moved, is not level or is past its calibration due date.
- Do not lean on the weighing table during weighing.
STAGE 2
Weighing
- 1Close the draught shield and zero the balance.
- 2Pass the container through the ioniser, then place it centrally on the pan with forceps. Close the doors and tare.
- 3Open the doors, add the sample with a micro-spatula, and close the doors again.
- 4Wait for the stability symbol. At this level it can take 10–30 seconds or more.
- 5Print or transfer the stable reading. Check the net weight is at or above the working minimum weight.
- Handle containers with forceps or gloves only. A fingerprint can weigh several micrograms.
- Do not breathe on the balance or reach into the chamber while the reading is settling.
- Use small, light containers so the tare does not use up most of the capacity.
STAGE 3
After use
- 1Remove the container and clean the pan and chamber with a soft brush.
- 2Close the doors and leave the balance on standby.
- 3Complete the usage log.
- Clean spills of potent powders immediately using the approved procedure; never blow powder out of the chamber.
In LimsPulse · Calibration Management
Keep every Microbalance in control: usage logs, calibration and maintenance schedules, and automatic blocking of overdue instruments.