Analytical balance · Calibration procedure
Linearity
Weighs several calibrated weights across the range, from low to near full capacity, and checks each reading is correct.

PURPOSE
Why this is checked
A balance adjusted at one point can still read wrongly at other loads. Linearity confirms it reads true across the whole range you use.
Frequency
Typically every 6 or 12 months, and after repair, relocation or a failed daily check, as defined in your calibration SOP.
Learn how the Analytical balance worksYOU WILL NEED
Standards & tools
- Set of calibrated weights covering the range, e.g. 50 g, 100 g, 150 g and 200 g (OIML class E2), with certificates
BEFORE YOU START
Prerequisites
- Balance level, clean and warmed up
- Weights at room temperature
PROCEDURE
Step by step
- 1Zero the balance.
- 2Weigh each test weight in turn, from the smallest to the largest, placing it in the centre of the pan.
- 3Record each stable reading and return to zero between weights.
- 4Calculate the difference between each reading and the certified value.
RECORD
Example observation table
| Certified value (g) | Observed (g) | Difference (g) | % error |
|---|---|---|---|
| 50.0000 | 50.0001 | +0.0001 | +0.0002% |
| 100.0000 | 100.0002 | +0.0002 | +0.0002% |
| 150.0000 | 150.0002 | +0.0002 | +0.00013% |
| 200.0000 | 200.0003 | +0.0003 | +0.00015% |
CALCULATION
How to calculate the result
Difference = Observed − Certified value; % error = Difference ÷ Certified value × 100
- 150 g weight reads 150.0002 g
- Difference = 0.0002 g
- % error = 0.0002 ÷ 150 × 100 = 0.00013%
ACCEPTANCE CRITERIA
Pass if
- Each difference within the manufacturer's linearity specification or the limit in your SOP (commonly within ±0.10% of the load, often with a tighter absolute limit).
IF IT FAILS
What to do
- Repeat after checking the environment and the weights.
- If it still fails, label the balance 'Out of calibration' and call service for adjustment.
- Assess results since the last passing calibration.
MORE
Other Analytical balance calibrations
In LimsPulse · Calibration Management
LimsPulse schedules this calibration, records the result against limits, and blocks the instrument everywhere if it fails or goes overdue.