LimsPulse
Vicat · Calibration procedure

Needle and plunger dimension check

Measures the plunger, initial and final setting needles, mould and moving mass of the Vicat apparatus and checks them against the specified dimensions.

Photo of a Vicat
Photo: Habib M’henni, CC BY-SA 3.0 (cropped), via Wikimedia Commons
PURPOSE

Why this is checked

Consistency and setting time depend on the exact size of the plunger and needles and on the mass of the moving part. A worn or bent needle, or a wrong total mass, changes penetration and gives false setting times.

Frequency

Typically every 6 to 12 months, and whenever a needle is replaced or appears bent, as defined in your SOP.

Learn how the Vicat works
YOU WILL NEED

Standards & tools

  • Calibrated digital vernier calliper (0.01 mm resolution)
  • Calibrated micrometer (0.001 mm or 0.01 mm resolution) for needle section
  • Calibrated balance (0.1 g or better)
  • Calibrated steel rule for scale check
BEFORE YOU START

Prerequisites

  • Attachments clean and dry
  • Apparatus on a level surface
PROCEDURE

Step by step

  1. 1Measure the plunger diameter at three positions and its length.
  2. 2Measure the initial setting needle section (side of the square, or diameter) near the tip and at mid-length, and its length; check it is straight.
  3. 3Measure the final setting needle: collar diameter and how far the needle tip projects beyond the collar.
  4. 4Weigh the moving rod with each attachment fitted to find the total moving mass.
  5. 5Check the scale reads zero with the plunger resting on the base plate and that graduations agree with a calibrated rule.
  6. 6Measure mould height and internal diameters at top and bottom.
  7. 7Record all values against the specified dimensions.
RECORD

Example observation table

ItemSpecified (typical)MeasuredResult
Plunger diameter10 mm10.02 mmPass
Plunger length50 mm50.1 mmPass
Initial needle section1 mm (square, IS)1.01 mmPass
Final needle collar diameter5 mm5.02 mmPass
Needle projection beyond collar0.5 mm0.50 mmPass
Total moving mass300 g300.2 gPass
Mould height40 mm40.1 mmPass
CALCULATION

How to calculate the result

Formula
Deviation = Measured − Specified; compare |Deviation| with the tolerance in the apparatus standard or SOP
Worked example
  1. 1
    Plunger diameter measured at three points: 10.01, 10.02, 10.03 mm; mean = 30.06 ÷ 3 = 10.02 mm
  2. 2

    Deviation = 10.02 − 10.00 = +0.02 mm, within a typical tolerance of ±0.05 mm

  3. 3

    Moving mass 300.2 g: deviation +0.2 g, within a typical tolerance of ±0.5 g (as in ASTM C187 / C191)

ACCEPTANCE CRITERIA

Pass if

  • Each dimension and the moving mass within the tolerances of the apparatus standard (IS 5513 / ASTM C187 and C191) or your SOP; typical values: plunger 10 mm × 50 mm, initial needle about 1 mm section, collar about 5 mm with 0.5 mm needle projection, moving mass 300 g.
  • Needle straight, tip square and free from burrs; rod slides freely.
IF IT FAILS

What to do

  • Replace any needle or plunger out of tolerance, bent or worn.
  • Adjust or replace the moving rod if the mass is out of tolerance.
  • Assess consistency and setting-time results since the last satisfactory check.
In LimsPulse · Calibration Management

LimsPulse schedules this calibration, records the result against limits, and blocks the instrument everywhere if it fails or goes overdue.

See how